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Exposure of an enone to a catalytic quantity of [CuH(PPh 3 )] 6 in the presence of one of several silyl hydrides (PhMe 2 SiH, PMHS, HMe 2 SiOSiMe 2 H) leads to conjugate reduction with concomitant formation of the corresponding silyl enol ether. Without isolation, treatment of these intermediates with a Lewis acid at low temperatures in the presence of an aldehyde,...
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