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A novel scheme has been proposed by computational methods (B3LYP and CCSD(T)) to produce hydroxylamine under normal experimental conditions using [O3Re‐(NH2)] and H2O2 under basic conditions. This particular reaction may proceed similar to Baeyer–Villiger oxidation and μ‐peroxo type pathways to insert oxygen into the ReNH2 bond to yield NH2OH; nevertheless, Baeyer–Villiger type oxidation is seems...
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