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Synthetically valuable chiral (aziridin‐2‐yl)oxirane‐3‐carbaldehydes bearing three consecutive functional groups including aziridine, epoxide, and aldehyde were prepared from the stereoselective epoxidation of (aziridin‐2‐yl)acrylaldehydes with H2O2 using organocatalyst (2R)‐ or (2S)‐[diphenyl(trimethylsilyloxy)methyl]pyrrolidine as organocatalyst. The regioselective ring opening of aziridines and...
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