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The novel free radical‐based cleavage of the enaminone C=C double bond is realized by using N‐halosuccinimides (NXS) in the presence of benzoyl peroxide (BPO) with mild heating, enabling the tunable synthesis of α,α‐dihalomethyl ketones and α,α,α‐trihalomethyl ketones under different reaction conditions. The formation of these divergent products involving featured C=C double bond cleavage requires...
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