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A facile route to reassemble titania nanoparticles within the titania‐block copolymer composite films has been developed. The titania nanoparticles templated by the amphiphilic block copolymer of poly(styrene)‐block‐poly (ethylene oxide) (PS‐b‐PEO) were frozen in the continuous PS matrix. Upon UV exposure, the PS matrix was partially degraded, allowing the titania nanoparticles to rearrange into chain‐like...
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