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The single phase LiNiVO4 has been successfully synthesized by adopting a new mild liquid route with oxalic acid as both complexant and precipitant, and this method is named the CPG method. The products were obtained by sintering the dry gel precursor which was prepared by the CPG method at 200–850 °C for 2–10 h in air. The products were tested by XRD, XPS, ESR and TGA-DTA, and the results indicate...
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