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Previous studies describe derivatization of metal ions followed by analysis using gas chromatography, usually on packed columns. In many of these studies, stable and volatile derivatives were formed using fluorinated β‐diketonate reagents. This paper extends previous work by investigating separations of the derivatives on small‐diameter capillary gas chromatography columns and exploring on‐fiber,...
DOI: 10.1002/jssc.201200537Europium(III) derivative formed by reaction of the europium ion with a fluorinated β‐diketonate reagent and a neutral donor. The resulting non‐polar, thermally stable, and luminescent derivative partitions into cyclohexane upon formation and can be subjected to high‐resolution capillary gas chromatography. This approach is used to separate derivatives of lanthanides that...
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