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The bayerite-derived layered double hydroxide of Li and Al crystallizes in a hexagonal structure (space group P3¯1m) on temperature induced dehydration. The metal hydroxide layers are stacked one above another [stacking vector (0, 0, 1)] in this crystal and the nitrate ion is intercalated with its molecular plane parallel to the metal hydroxide layer. On hydration, (i) there is an expansion in the...
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