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•AgInZn7S9 nanorods with a diameter of about 7nm was synthesized through a modified high-temperature pyrolysis method. •Hydrophobic AgInZn7S9 were transfered into water by surfactants with different charge types for photocatalytic H2 evolution. •Negatively charged surfactants inserted into the hydrophobic layer of AgInZn7S9 can enrich protons in water via electrostatic interactions around photocatalysts...
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