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Polyphenolic aglycones featuring two sugars individually attached via C‐glycosidic linkage (di‐C‐glycosides) represent a rare class of plant natural products with unique physicochemical properties and biological activities. Natural scarcity of such di‐C‐glycosides limits their use‐inspired exploration as pharmaceutical ingredients. Here, we show a biocatalytic process technology for reaction‐intensified...
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