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The highly sensitive detection of carcinogenic pollutant 2,4,6‐trinitrophenol (PA) is of great significance for environmental protection and human health. Based on the organic building block 1,3,6,8‐tetrakis (p‐benzoic acid) pyrene (H4TBAPy), the porous nano‐scale hydrogen‐bonded organic framework material (PFC‐1) was successfully synthesized. The large π‐π conjugated structure makes it to show excellent...