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The kinetics, mass transport, and double layer features of the reversible ferro-ferricyanide redox couple were studied through intermodulated differential immittance spectroscopy (IDIS). The system is fully characterized by the quantification of the electron-transfer parameters (α, and i0), the diffusion coefficients of the redox couple (Dred and Dox), together with the double layer capacitance and...
The use of intermodulated nonlinear analysis is important in the study of electrochemical systems, in order to separate the effects of kinetic (α, and i0), mass transport (Dred and Dox), and capacitive contributions within a single measurement at open circuit potential. The advantage of such treatment is that no assumption on the potential dependence of the parameters is required. In this paper, the...
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