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A first example of Fe‐catalyzed dearomative amination of β‐naphthols with aryl azides is described. The method constructs a nitrogen‐containing quaternary carbon center catalyzed by cheap and readily available iron salt FeCl2, and affords a series of α‐amino‐β‐naphthalenones in good to excellent yields under simple and mild reaction conditions. Preliminary experimental and computational studies suggest...
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