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Coherent anti‐Stokes Raman scattering (CARS) spectroscopy is applied to diagnostics of phase behavior of a fluid in pores of nanoporous glasses. Samples with mean pore radii of 2 and 3.5 nm were filled with compressed carbon dioxide at near‐room temperatures. CARS spectra of the 1388 cm−1 Q‐branch were measured at isothermal compressing in a wide pressure range including the transition from gaseous...
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