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Solid solution Zn2−2xCu2xSiO4 with the willemite structure has been synthesized by the proposed solid-phase synthesis procedure. It is shown that the maximum annealing temperature is 1030 ± 1°C because of the decomposition of CuO. The extent of the Zn2−2xCu2xSiO4 solid solution is 7.5 at % Cu. The unit cell crystal-chemical parameters and coefficients of thermal linear and volume expansion are independent...
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