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Three novel oligosaccharides of human infant faeces have been fully characterised by methylation analysis and 500/600 MHz 1 H NMR spectroscopy including DQF-COSY, TQF-COSY, TOCSY and ROESY experiments. The oligosaccharides were shown to be lactose-based structures two of which were substituted at C-6 of Gal with either the Le x trisaccharide, Gal(β 1-4)[Fuc(α 1-3)]GlcNAc(β 1-, or...
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