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This work is aimed to synthesize anhydrous Li2B12H12 with high purity via solvent-free reaction between solid state reagents LiBH4 and B10H14. The reaction is conducted respectively in open system and sealed system for comparison. It is observed to experience three thermodynamic steps: (1) melting of B10H14 at 103°C, (2) phase transition of LiBH4 at 118°C and (3) Li2B12H12 formation at 135°C. With...
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