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A novel silicon‐containing resin (ESA resin) was successfully synthesized by the condensation reaction of lithium arylacetylide with chlorosilane in high yields. The resin was characterized by the techniques of FTIR, 1H‐NMR, 29Si‐NMR, and gel permeation chromatography. Thermal cure process was monitored by DSC and FTIR methods. This resin could melt at around 100°C and thermally cured at 200–250°C...
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