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Fe-Co nanoparticles were prepared by mechanical alloying in air with various milling times from 0 h to 10 h and annealing temperatures in the range from 773 K to 973 K. The combined use of both conventional x-ray diffraction (XRD) and synchrotron x-ray absorption spectroscopy (XAS) techniques allowed us to obtain accurate data on the phase formation and the oxidation state of the materials. XRD patterns...
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