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Controllable modulation of the stacking modes of 2D (two‐dimensional) materials can significantly influence their properties and functionalities but remains a formidable synthetic challenge. Here, an effective strategy is proposed to control the layer stacking of imide‐linked 2D covalent organic frameworks (COFs) by altering the synthetic methods. Specifically, a modulator‐assisted method can afford...
Covalent organic frameworks (COFs) are an emerging class of porous crystalline polymers with well‐defined structures and tunable functionalities, which have fascinating applications in a wide range of fields. However, the synthetic procedures of COFs are mainly confined to the solvothermal synthesis method which usually requires harsh experimental conditions. In this work, an effective solvent‐free...
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