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Boron-containing CaAl-layered double hydroxides (LDHs) were prepared by milling, as well as the dehydration–rehydration and the anion-exchange methods. The substances obtained were structurally characterized by powder X-ray diffraction measurements, scanning electron microscopy and infrared spectroscopy. Various borate species could be introduced among the layers and/or the outer surface of the CaAl-LDH...
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