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The thermal behavior of ammonium molybdates, i.e., (NH4)6Mo7O24·4H2O (1) and (NH4)2MoO4 (2), was studied in inert (N2) and oxidizing (air) atmospheres by TG/DTA-MS, XRD, FTIR and SEM. The thermal decomposition sequence of 2 had similarities to 1; however, there were significant differences as well. When both of them were annealed, NH3 and H2O were released parallel, and in air the as-evolved NH3 was...
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