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Fe 50−x Cu 50−x B 2x alloy was obtained by an aqueous chemical reduction at pH=7.0, using fast and slow NaBH 4 solution addition methods. According to X-ray diffraction patterns, TEM and HRTEM observations, smaller than 10 nm nanocrystals of fcc-FeCuB were formed when the fast method was employed. The room temperature Mössbauer spectrum of this FeCuB nanoalloy shows...
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