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Infrared spectroscopic studies have been carried out to address the question of the Cu+ cation migration from hexagonal prisms (SI) and cubooctahedra (SI′) to supercages upon adsorption of ethene and ethyne in CuNaY and CuNaX zeolites. The quantitative assessment of Cu+ content in supercages before ethene and ethyne adsorption was evaluated on the basis of carbon monoxide adsorption experiments and...
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