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The effects of ZrO2 particle size (55 nm and 113 nm) and borothermal reduction routes (borothermal reduction with water‐washing (BRW) and in situ 5 mol% TaB2 solid solution, BRS) on synthesis and densification of ZrB2 were investigated. Irrespective of reduction routes, the use of finer ZrO2 powders as raw materials resulted in finer ZrB2 powders. Compared to the powders derived from BRS, the powders...