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In this work, disposable thick‐film copper electrodes were used for the detection of malachite green by Electrochemical Surface‐Enhanced Raman Spectroscopy (EC‐SERS). In situ real‐time SERS detection of malachite green was performed during the activation of copper electrodes by voltammetry. This time‐resolved method allowed to find dynamically the optimal potential where the detection sensitivity...
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