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1,4,5,8,9,12‐Hexaazatriphenylene (HAT) is one of the smallest polyheterocyclic aromatic building blocks for forming conjugated metal–organic frameworks (cMOFs). However, the strong inter‐molecular steric hindrance impedes the growth of HAT‐based cMOFs. Here we employ on‐surface synthesis to grow single‐layer two‐dimensional cMOFs of M3(HAT)2 (M=Ni, Fe, Co). Using scanning tunnelling microscopy and...
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