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Fluorinated steroids were examined using 1D and 2D homo‐ and heteronuclear 19F NMR, such as 19F1H and 19F13C. The utilization of fluorine NMR accounted for spectral simplification and resulted in a straightforward pathway for the determination of structures including the configuration of these compounds; these steroids present an illustrative example for other types of fluorinated compounds, which...
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