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A new three‐dimensional (3D) framework, [Ni(btzip)(H2btzip)]⋅2 DMF⋅2 H2O (1) (H2btzip=4,6‐bis(triazol‐1‐yl)isophthalic acid) as an acidic heterogeneous catalyst was constructed by the reaction of nickel wire and a triazolyl‐carboxyl linker. Framework 1 possesses intersected 2D channels decorated by free COOH groups and uncoordinated triazolyl N atoms, leading to not only high CO2 and C2H6 adsorption...
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