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A new method used to obtain α,ω-carboxyl terminated oligo(butyl methacrylate) (di-CTBMA) is introduced in this paper, which combines a conventional solution free-radical polymerization and a chemical modification, i.e. saponification. Here, a ω-carboxyl terminated oligo(butyl methacrylate) (CTBMA) is firstly synthesized by a solution polymerization in tetrahydrofuran, where 4,4 ' -azobis(4-cyanovaleric...
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