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Micelle forming polymerized N-Undecylenyl-L-aminoacid and N-Undecylenyl-L-peptide derivatives have been obtained. These compounds are effective as pseudostationary phases in electrokinetic capillary electrophoresis for racemate resolution. Synthetic procedures are described in detail, as well as preliminary analytical data comparing aminoacid derivatives and an aminoacid derivative with a peptide...
The synthesis of a novel water-soluble chiral N-acylcalix(4)arene amino acid derivative has been achieved. The chiral calix(4)arene is in a “cone” conformation according to NMR spectroscopy. We report preliminary results using this chiral calixarene derivative as a mobile phase additive in capillary electrophoresis.
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