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In this study, we examine the effect of duty cycles (33%, 50% and 67%) under square-wave galvanostatic pulses on the electrodeposition of zinc-nickel-alumina (ZnNiAl2O3) composites from a sulfate bath. XRD results showed that the dominant phases of the ZnNiAl2O3 electrodeposits were mixtures of Zn21Ni5 and Zn22Ni3 phases together with as Al2O3. The Ni content measured in the electrodeposits using...
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