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A sensitive amine‐responsive disassembly of self‐assembled AuI‐CuI double salts was observed and its utilization for the synergistic catalysis was enlightened. Investigation of the disassembly of [Au(NHC)2][CuI2] revealed the contribution of Cu‐assisted ligand exchange of N‐heterocyclic carbene (NHC) by amine in [Au(NHC)2]+ and the capacity of [CuI2]− on the oxidative step. By integrating the implicative...
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