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The heterometallic complex CoRu(CO)7(μ-PPh2) (1) reacts with the diphosphine ligand (Z)-Ph2PCH=CHPPh2 under both thermolysis and Me3NO activation to furnish CoRu(CO)5[(Z)-Ph2PCH=CHPPh2](μ-PPh2) (2) in good yield. Treatment of 2 with dimethyl acetylenedicarboxylate (DMAD) at elevated temperature leads to the formal insertion of the DMAD ligand into the Co–phosphido bond and formation of the metallocyclic...
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