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Two new salts, [BzTPP]2[Cu(mnt)2] (1) and [4NO2BzTPP]2[Cu(mnt)2] (2) (BzTPP+ = benzyltriphenylphosphonium and mnt2− = maleonitriledithiolate) have been prepared and characterized by elemental analyses, UV, IR, molar conductivity and single-crystal X-ray diffraction. The single-crystal structure analysis shows that 1 crystallizes in the monoclinic space group P21/n, while 2 crystallizes in the triclinic...
The [MoO0.75S3.25Cu3Cl(bipy)2] complex was synthesized for nonlinear optical studies by the reaction of (NH4)2[MoOS3], CuCl and bipy in CH2Cl2 solution. A single crystal X-ray analysis revealed that the complex consists of a nest-shaped core. The Mo atom is tetrahedrally coordinated by four S atoms, or three S atoms and one terminal O atom. There are two types of copper atom in the MoO0.75S3.25Cu3...
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