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We report the large-scale synthesis of monodisperse Ag nanoparticles and their homogeneous assembly into TiO 2 nanotube arrays (TNAs) for enhancing the visible-light photoelectrocatalytic (PEC) activity of the photoanodes. Electron beam irradiation reduction was used to synthesize monodisperse mesoporous Ag nanoparticles, composed of smaller nanocrystals, with the aid of PVP surfactant. Ag...
The use of TiO 2 nanotube arrays fabricated by anode oxidation of titanium sheets as a photoelectrocatalyst is limited by low surface activity owing to passive crystallization post-treatment. We report here on a vacuum assisted filling route for modifying TiO 2 nanotube arrays using high-activity anatase TiO 2 nanoparticles as a filling. Photoelectrocatalytic degradation experiments...
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