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In artificial photocatalytic hydrogen evolution, effective incident photon absorption and a high‐charge recombination rate are crucial factors influencing the overall efficiency. Herein, a traditional solid‐state synthesis is used to obtain, for the first time, novel samples of few‐layered g‐C3N4 with vertically aligned MoS2 loading (MoS2/C3N4). Thiourea and layered MoO3 are chosen as precursors,...
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