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The formation of titanium nitride with rock salt structure (δ-TiN x ) was studied by mechanical milling of a mixture of Ti and hexagonal boron nitride (h-BN) powders and isothermal annealing of the mixture after milling for 70h under argon atmosphere. The mole ratio of Ti to h-BN is 22:78. In the milling process, an amorphous Ti–N alloy was formed firstly by a diffusion reaction between Ti...
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