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A solid state NMR experiment is introduced for probing motions on the millisecond time scale, based on dephasing and refocusing 1 H– 13 C or 1 H– 15 N dipolar couplings. The method is related to the previously described Centerband-Only Detection of Exchange or CODEX experiment. The use of an R-type dipolar recoupling sequence takes advantage of the strong 1 ...
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