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Hierarchical Fe5(PO4)4(OH)3·2H2O microflower was synthesized by a hydrothermal reaction with self-prepared β-FeOOH nanorod as raw material. The microflowers were self-assemblies of symmetric building blocks with deep grooves. The possible morphology evolution process was proposed. The microflowers morphology was retained when they were lithiated to prepare LiFePO4/C composites through a carbothermal...
An improved solid-state reaction route has been employed to synthesize Mg2+-doped LiFePO4/C nanocomposite cathode by calcining the precursor obtained via evaporating the mixture of ascorbic acid, LiCH3COO·2H2O, Mg(CH3COO)2·4H2O, and amorphous FePO4 nanoparticles in anhydrous ethanol under continuous stirring. Ascorbic acid used here acted as both reducing agent and carbon source. The amorphous FePO...
LiFePO4/C composite cathode material has been synthesized by a carbothermal reduction method using β-FeOOH nanorods as raw materials and glucose as both reducing agent and carbon source. The results indicate that the content of carbon and the morphology of raw material have effect on the electrochemical performance of the final LiFePO4/C material. Sample LFP14 with a carbon content of 2.79 wt.% can...
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