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The electroreduction behavior of bromostyrenes 1 in DMF has been detected by cyclic voltammetry (CV) on GC and Ag electrodes. Under the atmospheric pressure of CO2, selective electrocarboxylation of 1 was carried out in an undivided cell at Ag cathode under potentiostatic conditions, with the corresponding vinyl-benzoic acid methyl ester 3 as the principal product, accompanied by styrene 2. Moderate...
A simple and efficient electrocarboxylation reaction of aliphatic halides has been developed using silver as cathode, magnesium as anode and CH 3 CN saturated CO 2 as solvent in an undivided cell. The influence of some key factors (such as the nature of electrode materials, supporting electrolytes and temperature) on this reaction was investigated. Under the optimized condition, the...
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