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The facile and convenient preparation of both enantiomers of a [7]helicene scaffold from inexpensive (l)‐(+)‐tartaric acid and 4‐methylstyrene is described. These helical structures were transformed into bis‐iodinated ether derivatives in order to explore their potential as precursors of novel chiral organoiodane reagents or as iodoarene pre‐catalysts. Promising results were obtained in hydroxylative...
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