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The cubic phase LiMn 2 O 4 spinel is synthesized via a directly soft chemistry method via hydrothermal reaction of Mn(NO 3 ) 2 , LiOH and H 2 O 2 at 383K for 5–10h, more favorable to control the nanocrystalline structure with well-defined pore-size distribution and high surface area than traditional solid-phase reaction at high temperature. Further,...
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