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The salt [HNEt 3 ][7-nido-SB 10 H 11 ] isolated from the room temperature reaction between B 10 H 14 , elemental S and NEt 3 by the method of Štíbr and co-workers is essentially pure. The salt has been structurally characterised by X-ray diffraction and its 11 B NMR spectrum fully assigned, correcting a previous mis-assignment. Deprotonation...
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