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A neutron diffraction study was carried out on metastable FCC and HCP phases in the Fe–Mn–Si system using small pieces of material inside a rotating device to simulate a polycrystalline randomly oriented sample. The experiments were performed on a set of Fe–Mn–Si alloys (16at.%≤C Mn ≤32at.% and 0at.%≤C Si ≤12at.%). FCC and HCP phases were retained at room temperature by a fast quench...
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