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Variable size sulfur aggregates (S n with 3≤n≤8) were investigated in the S 2p excitation regime (160 eV≤E≤175 eV) using monochromatic synchrotron radiation. Partial ion yields of mass-selected cations are compared with semiempirical extended Hückel calculations, yielding detailed information on the electronic and geometric structure of the aggregates. Inner-shell excitation in the S 2p regime...
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