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The α-Zn2P2O7 compound was obtained by conventional solid-state reaction. The sample was characterized by X-ray powder diffraction, solid state 31P NMR MAS, and electrical impedance spectroscopy. The solid state 31P MAS NMR, performed at 121.49 MHz, shows three isotropic resonances at −21.1, −18.8, and −15.8 ppm, confirming the non-equivalency of the three PO4 groups in the α-Zn2P2O7 form. They are...
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