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A series of Nd and Ce co-doped (Gd1−xNdx)2(Zr1−xCex)2O7 (0 ≤ x ≤ 1) pyrochlores were synthesized by flux method at 900–1000°C using nitrates as starting materials and a small amount of NaF as fluxing agent. The influences of contents of Nd/Ce, fluxing agent and reaction temperature on the phase structure of the pyrochlores were systematically investigated by X-ray diffraction (XRD) and Raman spectroscopy...
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