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The current work reports single‐phase, terbium‐doped sodium dysprosium fluoride (NaDyF4:Tb3+) nanocrystals with green luminescence and good T2 contrast in 7.0‐T MRI phantom and animal imaging. The current nanocrystals demonstrate good potential as a dual modal contrast agent for high‐field magnetic resonance (MR) and fluorescence imaging.
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