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A layered metal‐organic framework Zn‐TPN was designed and fabricated by solvothermal reaction. The crystal structure was a lamellar structure, and the unique coordination pattern provided Lewis acid sites that could be employed as efficient catalytic sites. Zn‐TPN displayed a satisfactory catalytic effect for Knoevenagel condensation of malononitrile and benzaldehyde. At 75 °C, the conversion rate...